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Beilstein J. Org. Chem. 2019, 15, 2563–2568, doi:10.3762/bjoc.15.249
Graphical Abstract
Figure 1: Structure of the target pentasaccharide repeating unit in the form of its 2-aminoethyl glycoside.
Figure 2: Retrosynthetic analysis for the synthesis of the target pentasaccharide 1.
Scheme 1: Synthesis of the disaccharide acceptor 5.
Scheme 2: Synthesis of the trisaccharide acceptor 11.
Scheme 3: Synthesis of the non-reducing end disaccharides (16a and 16b).
Scheme 4: Synthesis of the target pentasaccharide 1.